Restor Dent Endod.  2019 Nov;44(4):e45. 10.5395/rde.2019.44.e45.

Influence of 10-MDP concentration on the adhesion and physical properties of self-adhesive resin cements

Affiliations
  • 1Department of Operative Dentistry, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences, Okayama, Japan. shibuya-k@okayama-u.ac.jp

Abstract


OBJECTIVES
Self-adhesive resin cements contain functional monomers that enable them to adhere to the tooth structure without a separate adhesive or etchant. One of the most stable functional monomers used for chemical bonding to calcium in hydroxyapatite is 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP). The aim of this study was to evaluate the influence of the10-MDP concentration on the bond strength and physical properties of self-adhesive resin cements.
MATERIALS AND METHODS
We used experimental resin cements containing 3 different concentrations of 10-MDP: 3.3 wt% (RC1), 6.6 wt% (RC2), or 9.9 wt% (RC3). The micro-tensile bond strength of each resin cement to dentin and a hybrid resin block (Estenia C&B, Kuraray Noritake Dental) was measured, and the fractured surface morphology was analyzed. Further, the flexural strength of the resin cements was measured using the three-point bending test. The water sorption and solubility of the cements following 30 days of immersion in water were measured.
RESULTS
The bond strength of RC2 was significantly higher than that of RC1. There was no significant difference between the bond strength of RC2 and that of RC3. The water sorption of RC3 was higher than that of any other cement. There were no significant differences in the three-point bending strength or water solubility among all three types of cements.
CONCLUSIONS
Within the limitations of this study, it is suggested that 6.6 wt% 10-MDP showed superior properties than 3.3 wt% or 9.9 wt% 10-MDP in self-adhesive resin cement.

Keyword

Flexural strength; Resin cements; 10-methacryloyloxydecyl dihydrogen phosphate; Tensile bond strength; Water solubility; Water sorption

MeSH Terms

Adhesives
Calcium
Dentin
Durapatite
Immersion
Resin Cements*
Solubility
Tooth
Water
Adhesives
Calcium
Durapatite
Resin Cements
Water
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